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Thermal Conductivity Measurements of diamond thin films by 3ω-method (CAT#: STEM-PPA-0043-WXH)

Introduction

Progress made in the last two decades in chemical vapour deposition technology has enabled the production of inexpensive, high-quality coatings made from diamond to become a scientific and commercial reality. Two properties of diamond make it a highly desirable candidate material for biomedical applications: first, it is bioinert, meaning that there is minimal immune response when diamond is implanted into the body, and second, its electrical conductivity can be altered in a controlled manner, from insulating to near-metallic. In vitro, diamond can be used as a substrate upon which a range of biological cells can be cultured. In vivo, diamond thin films have been proposed as coatings for implants and prostheses.




Principle

The process involves a metal heater applied to the sample that is heated periodically. The temperature oscillations thus produced are then measured. The thermal conductivity and thermal diffusivity of the sample can be determined from their frequency dependence.

Applications

Determining the thermal conductivities of bulk material (i.e. solid or liquid) and thin layers

Procedure

1. Sample preparation and mounting
2. Experimental condition setting
3. Experiment start: Turn on the 3ω signal generator and lock-in amplifier, and control the temperature controller to make the sample temperature reach the set value. When the sample reaches a stable state, data acquisition and processing begin.
4. Data processing