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Determination of Water Content of Crude Oil by Azeotropic Distillation (CAT#: STEM-PPA-0121-YJL)

Introduction

Water in crude oil can increase friction in pipelines and thus increase the energy cost of transportation. It can also dissolve salts, which accelerates the corrosion of refining equipment and the scaling of pipelines. Excessive water in crude oil increases the energy required during distillation and can cause instability in the refining operation. Therefore, the excessive water must be removed prior to refining, which consumes energy and reagents. The water content of crude oil must be determined accurately to ensure operational safety and economic efficiency.




Principle

Azeotropic distillation refers to a series of techniques that destroy the azeotropic composition in distillation to carry out distillation or fractionation, and use two organic solvents to form an azeotrope for distillation.
Azeotropic distillation, also known as azeotropic distillation, is to add a selected third component to the separated mixed liquid to form a new azeotrope with one or more components in the original mixture. And its boiling point is lower than that of any original component. In this way, the new azeotrope is distilled from the top of the column during distillation, while the bottom product is a pure component, thereby achieving the purpose of separating the original mixture.
Azeotropic distillation is suitable for separating mixed liquids with only azeotropic composition and relative volatility close to 1.

Applications

Food industry; Petroleum industry

Procedure

1. Add the sample to the still.
2. Add to collection bottle.
3. Heat.
4. Collect the liquid.
4. Calculate moisture content.

Materials

• Sample Type: liquid or powder