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Determination of Melting Point of Sn-Ag-Cu Solder Alloy on Cu Substrate by Instantaneous Method (CAT#: STEM-PPA-0119-YJL)

Introduction

There have been several regulations to ban Pb from electronic products all over the world. The European Union’s RoHS directive is the initial driving force for the elimination of Pb because Pb contained in conventional solder materials has harmful influence on the environment and human health. As a result, lead-free solders with microstructure stability and mechanical properties comparable with eutectic Pb–Sn solder stimulate immense interests in microelectronic application. Nowadays several lead-free solders including Sn-Ag, Sn-Cu, Sn-Zn, Sn-Ag-Bi and Sn-Ag-Cu systems have been developed. Among them, the near-ternary eutectic Sn-Ag-Cu system solders have been regarded as primary candidates because of their good mechanical and acceptable wetting properties as well as suitable melting points.




Principle

Melting point is a characteristic property of solid crystalline substance. It is the temperature at which the solid phase changes to the liquid phase. This phenomenon occurs when the substance is heated.
The instantaneous melting point is determined by repeated dropping of particles of a pulverized substance on the surface of a metal heating block, while the block is being heated (1C/min). The temperature at which the substance melts for the first time upon contact with the metal is recorded. Subsequently,the heating is stopped and during the following cooling phase the highest temperature is recorded at which instantaneous melting is no longer observed. The instantaneous melting emperature is calculated as the average of the two recorded temperatures.

Applications

Chemical industry; Cosmetic/pharmaceutical industry

Procedure

1. Heat up the block quickly.
2. Drop several particles of finely ground substance.
3. Record the temperature t1 and t2.
4. Calculate the melting point.

Materials

• Sample Type: crystalline compounds